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Phase Transformation of Anhydrous to Dihydrate Carbamazepine: Preparation and Comparative Characterization

FABAD journal of pharmaceutical sciences, 2023-10, Vol.48 (3), p.431-442

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Title:
Phase Transformation of Anhydrous to Dihydrate Carbamazepine: Preparation and Comparative Characterization
Author: Wadher, Kamlesh ; Raut, Vaishnavi ; Hirave, Keshav ; Trivedi, Sagar ; Umekar, Milind
Subjects: Aluminum ; Bioavailability ; Dissolution ; Fourier transforms ; NMR ; Nuclear magnetic resonance ; Polymorphism ; Scanning electron microscopy ; Spectrum analysis
Is Part Of: FABAD journal of pharmaceutical sciences, 2023-10, Vol.48 (3), p.431-442
Description: Te purpose of the present investigation was to compare various techniques for the formation of Carbamazepine dihydrate from anhydrates and also to discriminate crystal forms of Carbamazepine by Melting point, FTIR DSC, Powder X-ray difractometry analysis, NMR, scanning electron microscopy, solubility and intrinsic dissolution testing. [...]it is crucial to discover any probable hydrate form promptly in the process of development of drug (Tian, 2010). Scanning Electron Microscopy (SEM) The SEM was used to evaluate the solid state tran¬sition of CBZ A and its dihydrated sample residuals following solubility and dissolution experiments. A ZEISS EVO HD 15 scanning electron microscope was used to obtain SEM micrographs.
Publisher: Ankara: Hacettepe University Faculty of Medicine
Language: English;Turkish
Identifier: ISSN: 1300-4182
DOI: 10.55262/fabadeczacilik.1269595
Source: ProQuest Central

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