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Phase contrast scanning transmission electron microscopy imaging of light and heavy atoms at the limit of contrast and resolution

Scientific reports, 2018-02, Vol.8 (1), p.2676-10, Article 2676 [Peer Reviewed Journal]

2018. This work is published under http://creativecommons.org/licenses/by/4.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License. ;The Author(s) 2018 ;ISSN: 2045-2322 ;EISSN: 2045-2322 ;DOI: 10.1038/s41598-018-20377-2 ;PMID: 29422551

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  • Title:
    Phase contrast scanning transmission electron microscopy imaging of light and heavy atoms at the limit of contrast and resolution
  • Author: Yücelen, Emrah ; Lazić, Ivan ; Bosch, Eric G T
  • Subjects: Gallium ; Scanning electron microscopy ; Transmission electron microscopy
  • Is Part Of: Scientific reports, 2018-02, Vol.8 (1), p.2676-10, Article 2676
  • Description: Using state of the art scanning transmission electron microscopy (STEM) it is nowadays possible to directly image single atomic columns at sub-Å resolution. In standard (high angle) annular dark field STEM ((HA)ADF-STEM), however, light elements are usually invisible when imaged together with heavier elements in one image. Here we demonstrate the capability of the recently introduced Integrated Differential Phase Contrast STEM (iDPC-STEM) technique to image both light and heavy atoms in a thin sample at sub-Å resolution. We use the technique to resolve both the Gallium and Nitrogen dumbbells in a GaN crystal in [[Formula: see text]] orientation, which each have a separation of only 63 pm. Reaching this ultimate resolution even for light elements is possible due to the fact that iDPC-STEM is a direct phase imaging technique that allows fine-tuning the microscope while imaging. Apart from this qualitative imaging result, we also demonstrate a quantitative match of ratios of the measured intensities with theoretical predictions based on simulations.
  • Publisher: England: Nature Publishing Group
  • Language: English
  • Identifier: ISSN: 2045-2322
    EISSN: 2045-2322
    DOI: 10.1038/s41598-018-20377-2
    PMID: 29422551
  • Source: PubMed Central (Open access)
    ProQuest Central
    DOAJ Directory of Open Access Journals

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