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Scherrer grain-size analysis adapted to grazing-incidence scattering with area detectors

Journal of applied crystallography, 2009-12, Vol.42 (6), p.1030-1034 [Peer Reviewed Journal]

International Union of Crystallography, 2009 ;International Union of Crystallography 2009 2009 ;ISSN: 1600-5767 ;ISSN: 0021-8898 ;EISSN: 1600-5767 ;DOI: 10.1107/S0021889809040126 ;PMID: 19953189

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  • Title:
    Scherrer grain-size analysis adapted to grazing-incidence scattering with area detectors
  • Author: Smilgies, Detlef-M.
  • Subjects: Finite element analysis ; Grain size ; grazing-incidence small-angle scattering (GISAXS) ; grazing-incidence wide-angle scattering (GIWAXS) ; Research Papers ; Scattering ; Scherrer formula ; soft materials ; thin films
  • Is Part Of: Journal of applied crystallography, 2009-12, Vol.42 (6), p.1030-1034
  • Description: Ever since its formulation, the Scherrer formula has been the workhorse for quantifying finite size effects in X‐ray scattering. Various aspects of Scherrer‐type grain‐size analysis are discussed with regard to the characterization of thin films with grazing‐incidence scattering methods utilizing area detectors. After a brief review of the basic features of Scherrer analysis, a description of resolution‐limiting factors in grazing‐incidence scattering geometry is provided. As an application, the CHESS D1 beamline is characterized for typical scattering modes covering length scales from the molecular scale to the nanoscale.
  • Publisher: 5 Abbey Square, Chester, Cheshire CH1 2HU, England: International Union of Crystallography
  • Language: English
  • Identifier: ISSN: 1600-5767
    ISSN: 0021-8898
    EISSN: 1600-5767
    DOI: 10.1107/S0021889809040126
    PMID: 19953189
  • Source: Alma/SFX Local Collection

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